• |
It
may break under thermal stress in the ‘steady state’,that is when there
is established a constant thermal gradient through the glass. |
• |
It may break under the transient stress of a ‘thermalshock’ that is sudden heating or cooling |
• |
It may, if heated beyond certain temperature, acquire apermanent stress on cooling which could causesubsequent failure |
• |
The following advice will assist in avoiding failures during heating and cooling procedures: |
• |
Never leave vessel
unattended when evaporation work in being carried out. The vessel may
crack or explode as“dryness” condition is approached if the heat source
isas the liquid level drops |
• |
Always the caution when removing glassware from aheat source and avoid placing on a cold or damp surface |
• |
Although the ware can withstand extreme temperatures, sudden temperature changes may cause the vessel to break |
• |
Always cool vessels slowly to prevent thermal breakage |
• |
Never apply heat to badly scratched or etched vessel,as the thermal strength will have been greatly reduced |
• |
Never apply point source heating to a vessel, as this will greatly increase the chance of breakage |
• |
Always diffuse the
heat source by using a metal gauzeor air / water bath. Alternatively,
ensure even heating of the vessel by slow movement of the vessel in
relation to the heat source |
• |
Adjust Bunsen burner
to get a large soft flame. It will heat slowly but also more uniformly.
Uniform heat is critical factor for some chemical reactions |
• |
Ensures that the flame contacts the vessel below the liquid level. Heating above that level will invite breakage of the vessels |
• |
Always use
anti-bumping devices in the vessel, such as powdered pumice or glass
wool when rapid heating of the vessel and contents is required |
• |
Never use material with sharp edges such as broken
porcelain asan anti- bumping device. This will
causeinternalabrasionsand educe the mechanical and
thermal strength of the vessel. |